HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 66825660 | HCID 66825660 | — |
| Reactant | Tert-butyl 7-chloro-5-oxo-2,3-dihydroimidazo[1,2-C]pyrimidine-1(5H)-carboxylate | HCID 71743561 | — |
| Product | HCID 71243771 | HCID 71243771 | — |
Reaction Steps
Prepared in a manner similar to that described for E65 using NaH (11.04 mg, 0.276 mmol), (3-fluoro-4-(4-fluoro-3-(trifluoromethyl)phenoxy)-phenyl)methanol (56.0 mg, 0.184 mmol) and tertbutyl 7-chloro-5-oxo-2,3-dihydroimidazo[1,2-c]pyrimidine-1(5H)-carboxylate (50 mg, 0.18 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-3aea0808ede0437db2a9f3ecedbb427c |
| Source note | uspto-grants-2015_03 |