HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 63076546 | HCID 63076546 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71243757 | HCID 71243757 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using (4-(3,4-difluorophenoxy)-3,5-difluorophenyl)methanol (0.073 g, 0.269 mmol) in THF)(4 mL), sodium hydride (0.016 g, 0.404 mmol) and 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (0.050 g, 0.269 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-d1ed5854e4df4b8a8d598ca039ea2c9a |
| Source note | uspto-grants-2015_03 |