HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86724212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Reactant | HCID 86724213 | HCID 86724213 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86724212 | HCID 86724212 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (65 mg, 0.350 mmol), sodium hydride (22 mg, 0.550 mmol) and 2-((2-chloropyridin-4-yl)oxy)-5-(hydroxymethyl)benzonitrile (91 mg, 0.350 mmol) in DMF (2 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-c19a0a68e4fb49efa57076123040a304 |
| Source note | uspto-grants-2015_03 |