HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71243759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 71236710 | HCID 71236710 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 71243759 | HCID 71243759 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using 2-chloro-4-(2-cyano-4-(hydroxymethyl)phenoxy)benzonitrile (60 mg, 0.211 mmol) in THF (S mL), sodium hydride (12.64 mg, 0.316 mmol) and 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (39.1 mg, 0.211 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-9c2846d5f088428cbdb374f2de99ea65 |
| Source note | uspto-grants-2015_03 |