HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86724182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 53414454 | HCID 53414454 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86724182 | HCID 86724182 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using (3-chloro-4,5-difluorophen-yl)methanol (192 mg, 1.078 mmol) in DMF (4 mL), sodium hydride (129 mg, 3.23 mmol) and 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]pyrimidin-5(1H)-one (200 mg, 1.078 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-449f483bb0584371acf465dfcfe286e6 |
| Source note | uspto-grants-2015_03 |