HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 71241117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 71243819 | HCID 71243819 | — |
| Reactant | 7-Chloro-1-methyl-2,3-dihydroimidazo[1,2-C]pyrimidin-5(1H)-one | HCID 71743458 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 71241117 | HCID 71241117 | — |
Reaction Steps
Prepared in a manner similar to that described for E1 using 4-(2-fluoro-4-(hydroxymethyl)phenoxy)-2-methylbenzonitrile (1.00 g, 3.89 mmol) in DMF (10 mL), sodium hydride (0.280 g, 11.7 mmol) and 7-chloro-1-methyl-2,3-dihydroimidazo[1,2-c]p-yrimidin-5(1H)-one (0.721 g, 3.89 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975400B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-eb199f541a6a41129a737dfb0c4e5a9d |
| Source note | uspto-grants-2015_03 |