HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → HCID 86615121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | N-Boc-N-methylethylenediamine | HCID 2756424 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86615121 | HCID 86615121 | — |
Reaction Steps
To a well stirred solution of N-(tert-Butoxycarbonyl)-N-methyl-ethylenediamine 101 (5.5 g, 0.032 mol) in dichloromethane (CH2Cl2, 30 mL) was added succinic anhydride 102 (3.2 g, 0.032 mol) in one portion. After stirring the reaction mixture for 1 hour at room temperature, a slurry resulted. This slurry was used in Step 2 without further work-up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975404B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-163313e8e7c548d1af760c692a7ad068 |
| Source note | uspto-grants-2015_03 |