HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 86702121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | HCID 605909 | HCID 605909 | — |
| Solvent | 1,1,1,3,3,3-Hexafluoro-2-propanol | HCID 13529 | — |
| Product | HCID 86702121 | HCID 86702121 | — |
Reaction Steps
Ethyl 4-(4-nitrophenyl)-2,4-dioxobutanoate (500 mg, 1.885 mmol) was dissolved in hexafluoroisopropanol (4 ml) and methylhydrazine (87 mg, 1.885 mmol) was added dropwise. The reaction mixture was stirred at room temperature for 3 hours, concentrated to dryness, triturated with ether; and filtered to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975398B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-287f40f523cf4d39baddbff4b5db4974 |
| Source note | uspto-grants-2015_03 |