HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 117702727, compound → HCID 117702578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 117702727 | HCID 117702727 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 117702578 | HCID 117702578 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Example 1 using 4-((5-chloro-1-methyl-6-oxo-1,6-dihydropyridin-3-ylamino)(4-chlorophenyl)methyl)-1-(4-methoxy-benzyl)-1H-pyrazole-3-carboxylic acid (Step 9.5). tR: 4.58 min (HPLC 1); tR: 1.01 min (LC-MS 2); ESI-MS: 495/497 [M+H]+ (LC-MS 2); Rf=0.55 (CH2Cl2/MeOH 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-126c9088456e4f82b4f42f924be21815 |
| Source note | uspto-grants-2015_03 |