HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane methanol → 3-Chloro-5-iodo-1-methylpyridin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | HCID 178517798 | HCID 178517798 | — |
| Product | 3-Chloro-5-iodo-1-methylpyridin-2(1H)-one | HCID 23115960 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 23.2 using 3-chloro-5-iodo-pyridin-2-ol. tR: 3.30 min (HPLC 1); tR: 0.71 min (LC-MS 2); ESI-MS: 270 [M+H]+ (LC-MS 2); Rf=0.79 (CH2Cl2/MeOH 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-311a7e71d30e4dc686d6c7f1387f5846 |
| Source note | uspto-grants-2015_03 |