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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 873835Generated: October 30, 2026

Dichloromethane methanol → HCID 117702786, compound

https://huagongshe.com/reaction/873835

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethane methanolHCID 21226129—
ReactantHCID 117702780HCID 117702780—
ProductHCID 117702786HCID 117702786—

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)(1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-ylamino)methyl)-1-(4-methoxybenzyl)-5-methyl-1H-pyrazole-3-carboxylic acid (Step 27.2). tR: 4.54 min (HPLC 1); tR: 1.03 min (LC-MS 2); ESI-MS: 489 [M+H]+ (LC-MS 2); Rf=0.40 (CH2Cl2/MeOH 9:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08975417B2
Source datasetuspto-grants-2015_03
ORD IDord-0218af6b596b4bcfa4dccb9417c77a31
Source noteuspto-grants-2015_03