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HRID873847

反应详情

EQUATION

反应方程式

HRID 873847 的结构方程式

REACTANTS

反应物

2
结构：Cc1noc2ccc(N)cc12
HCID21345397

3-Methyl-1,2-benzoxazol-5-amine

C8H8N2O

结构：CCOC(=O)c1nn(C)c(C)c1C(O)c1ccc(Cl)cc1
HCID117702851

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nn(C)c(C)c1C(Nc1ccc2onc(C)c2c1)c1ccc(Cl)cc1
HCID117703133

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 1.4 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1,5-dimethyl-1H-pyrazole-3-carboxylate (Step 28.2) and 3-methylbenzo[d]isoxazol-5-amine (Step 33.3). tR: 5.40 min (HPLC 1); tR: 1.20 min (LC-MS 2); ESI-MS: 439 [M+H]+ (LC-MS 2); Rf=0.77 (CH2Cl2/MeOH 9:1).