HCID 117702781, compound → HCID 86294280, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-(((5-chloro-1-methyl-6-oxo-1,6-dihydropyridin-3-yl)amino)(4-chlorophenyl)methyl)-1-cyclopropyl-1H-pyrazole-5-carboxylic acid (Step 35.2). tR: 4.30 min (HPLC 1); tR: 0.98 min (LC-MS 2); ESI-MS: 415/417 [M+H]+ (LC-MS 2); Rf=0.33 (EtOAc); 1H NMR (400 MHz, DMSO-d6) δ ppm 0.99-1.10 (m, 2H) 1.17-1.30 (m, 2H) 3.42 (s, 3H) 3.83-3.94 (m, 1H) 6.11 (s, 1H) 7.21-7.29 (m, 2H) 7.32-7.38 (m, 2H) 7.41 (s, 1H) 7.88 (d, J=2.4 Hz, 1H) 7.92 (d, J=2.4 Hz, 1H).

Provenance & Evidence