HCID 117702678, compound → HCID 86294281, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)((1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)amino)methyl)-1-isopropyl-1H-pyrazole-5-carboxylic acid (Step 36.5). tR: 4.31 min (HPLC 1); tR: 0.97 min (LC-MS 2); ESI-MS: 397 [M+H]+ (LC-MS 2); Rf=0.22 (EtOAc); 1H NMR (400 MHz, DMSO-d6) δ ppm 1.47-1.56 (m, 6H) 1.91 (s, 3H) 3.34 (s, 3H) 4.73-4.87 (m, 1H) 6.09 (s, 1H) 7.18-7.25 (m, 2H) 7.32-7.38 (m, 3H) 7.40 (s, 1H) 7.71 (d, J=2.7 Hz, 1H).

Provenance & Evidence