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HRID873857

反应详情

EQUATION

反应方程式

HRID 873857 的结构方程式

REACTANTS

反应物

2
结构：Cn1cc(N)cc(Cl)c1=O
HCID71756073

未命名化合物

结构：CCOC(=O)c1nn(C2CC2)cc1C(O)c1ccc(Cl)cc1
HCID117702983

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nn(C2CC2)cc1C(Nc1cc(Cl)c(=O)n(C)c1)c1ccc(Cl)cc1
HCID117702599

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 10.3 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1-cyclopropyl-1H-pyrazole-3-carboxylate (Step 37.3) and 5-amino-3-chloro-1-methylpyridin-2(1H)-one (Step 5.2). tR: 4.54 min (HPLC 1); tR: 1.03 min (LC-MS 2); ESI-MS: 461 [M+H]+ (LC-MS 2); Rf=0.18 (EtOAc).