HCID 117702916, compound → HCID 86294478, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-(((5-chloro-1-methyl-6-oxo-1,6-dihydropyridin-3-yl)amino)(4-chlorophenyl)methyl)-1-isopropyl-1H-pyrazole-5-carboxylic acid (Step 38.2). tR: 4.55 min (HPLC 1); tR: 1.02 min (LC-MS 2); ESI-MS: 417 [M+H]+ (LC-MS 2); Rf=0.41 (EtOAc); 1H NMR (400 MHz, DMSO-d6) δ ppm 1.47-1.55 (m, 6H) 3.43 (s, 3H) 4.75-4.86 (m, 1H) 6.13 (s, 1H) 7.21-7.28 (m, 2H) 7.34-7.40 (m, 2H) 7.42 (s, 1H) 7.89 (d, J=2.7 Hz, 1H) 7.94 (d, J=2.7 Hz, 1H).

Provenance & Evidence