HCID 117702601, compound → HCID 86294481, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)((1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)amino)methyl)-1-isopropyl-1H-pyrazole-3-carboxylic acid (Step 41.5). tR: 4.05 min (HPLC 1); tR: 0.90 min (LC-MS 2); ESI-MS: 397 [M+H]+ (LC-MS 2); Rf=0.60 (CH2Cl2/MeOH 9:1); 1H NMR (400 MHz, DMSO-d6) δ ppm 1.38-1.47 (m, 6H) 1.90 (s, 3H) 3.34 (s, 3H) 4.54-4.65 (m, 1H) 6.12 (s, 1H) 7.17-7.24 (m, 2H) 7.30-7.39 (m, 3H) 7.69 (d, J=2.7 Hz, 1H) 7.85 (s, 1H).

Provenance & Evidence