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HRID873871

反应详情

EQUATION

反应方程式

HRID 873871 的结构方程式

REACTANTS

反应物

2
反应SMILES：Cn1cc(N)cc(Cl)c1=O
HCID71756073

未命名化合物

反应SMILES：CCOC(=O)c1nn(C(C)C)cc1C(O)c1ccc(Cl)cc1
HCID117702963

Ethyl 4-[(4-chlorophenyl)hydroxymethyl]-1-(1-methylethyl)-1H-pyrazole-3-carboxylate

C16H19ClN2O3

PRODUCTS

产物

1
反应SMILES：CCOC(=O)c1nn(C(C)C)cc1C(Nc1cc(Cl)c(=O)n(C)c1)c1ccc(Cl)cc1
HCID117702883

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCOC(C)=O
溶剂HCID8857

Ethyl Acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 10.3 using ethyl 4-((4-chlorophenyl)(hydroxy)methyl)-1-isopropyl-1H-pyrazole-3-carboxylate (Step 41.3) and 5-amino-3-chloro-1-methylpyridin-2(1H)-one (Step 5.2). tR: 4.65 min (HPLC 1); tR: 1.07 min (LC-MS 2); ESI-MS: 463 [M+H]+ (LC-MS 2); Rf=0.30 (EtOAc).