HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 117702959, compound → HCID 86294689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 117702959 | HCID 117702959 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86294689 | HCID 86294689 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Example 1 using 4-(((5-chloro-1-methyl-6-oxo-1,6-dihydropyridin-3-yl)amino)(4-chlorophenyl)methyl)-1-cyclopropyl-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid (Step 44.4).; tR: 1.16 min (LC-MS 2); ESI-MS: 483 [M+H]+ (LC-MS 2); Rf=0.61 (CH2Cl2/5% MeOH); 1H NMR (400 MHz, DMSO-d6) δ ppm 1.08-1.17 (m, 2H) 1.27-1.38 (m, 2H) 3.40 (s, 3H) 3.89-4.09 (m, 1H) 6.27 (s, 1H) 7.25-7.42 (m, 4H) 7.90 (d, J=2.7 Hz, 1H) 7.86 (d, J=2.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-44dcd3e12ac04f408184c95feb76bcf4 |
| Source note | uspto-grants-2015_03 |