HCID 117702697, compound → HCID 86294690, compound

Participants

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 1 using 4-((4-chlorophenyl)((1,5-dimethyl-6-oxo-1,6-dihydropyridin-3-yl)amino)methyl)-1-cyclopropyl-3-(trifluoromethyl)-1H-pyrazole-5-carboxylic acid (Step 45.2). tR: 1.13 min (LC-MS 2); ESI-MS: 463 [M+H]+ (LC-MS 2); Rf=0.61 (CH2Cl2/5% MeOH); 1H NMR (400 MHz, DMSO-d6) δ ppm 1.07-1.17 (m, 2H) 1.27-1.40 (m, 2H) 1.89 (s, 3H) 3.32 (s, 3H) 3.95-4.05 (m, 1H) 6.24 (s, 1H) 7.21-7.40 (m, 5H) 7.69 (d, J=2.7 Hz, 1H).

Provenance & Evidence