HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzaldehyde → HCID 117702714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | HCID 117702818 | HCID 117702818 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 117702714 | HCID 117702714 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 1.3 using ethyl 1-(2,4-dimethoxypyrimidin-5-yl)-4-iodo-3-methyl-1H-pyrazole-5-carboxylate (Step 52.2) and 4-chlorobenzaldehyde at RT for 30 min. tR: 5.02 min (HPLC 1); tR: 1.11 min (LC-MS 2); ESI-MS: 433 [M+H]+ (LC-MS 2); Rf=0.38 (hexane/EtOAc 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-c2f7d9c07d6e4a4f96ceab85d2203086 |
| Source note | uspto-grants-2015_03 |