HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzaldehyde → HCID 117702898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | HCID 117702787 | HCID 117702787 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 117702898 | HCID 117702898 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 1.3 using ethyl 4-iodo-1-(2-methoxypyrimidin-4-yl)-3-methyl-1H-pyrazole-5-carboxylate (Step 59.3) and 4-chlorobenzaldehyde at RT for 60 min. tR: 5.20 min (HPLC 1); tR: 1.18 min (LC-MS 2); ESI-MS: 403 [M+H]+ (LC-MS 2); Rf=0.44 (hexane/EtOAc 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-6aea32f9985e4036abc1a4ffe4ac7238 |
| Source note | uspto-grants-2015_03 |