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HRID873948

反应详情

EQUATION

反应方程式

HRID 873948 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccc(Cl)cc1
HCID7726

4-Chlorobenzaldehyde

C7H5ClO

结构：CCOC(=O)C(=O)CC(C)=O
HCID69208

Ethyl 2,4-dioxovalerate

C7H10O4

结构：Cc1cc(N)cn2c(C)nnc12
HCID75357449

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)C1=C(O)C(=O)N(c2cc(C)c3nnc(C)n3c2)C1c1ccc(Cl)cc1
HCID117702671

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 84.5 using 3,8-dimethyl-[1,2,4]triazolo[4,3-a]pyridin-6-amine (Step 67.4), 4-chlorobenzaldehyde and ethyl 2,4-dioxovalerate. tR: 0.70 min (LC-MS 2); ESI-MS: 397 [M+H]+ (LC-MS 2); 1H NMR (400 MHz, DMSO-d6) δ ppm 2.36 (s, 3H) 2.44 (s, 3H) 2.63 (s, 3H) 6.14 (s, 1H) 7.27 (d, J=8.4 Hz, 2H) 7.33-7.40 (m, 3H) 8.53 (s, 1H).