HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2,4-dioxovalerate → HCID 117702592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2,4-dioxovalerate | HCID 69208 | — |
| Reactant | p-(Trifluoromethoxy)benzaldehyde | HCID 69573 | — |
| Reactant | 5-Amino-1,3-dimethyl-1,2-dihydropyridin-2-one | HCID 67456616 | — |
| Product | HCID 117702592 | HCID 117702592 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 57.1 using 5-amino-1,3-dimethylpyridin-2(1H)-one (Step 20.2), 4-trifluoromethoxy-benzaldehyde and ethyl acetopyruvate. tR: 0.79 min (LC-MS 2); ESI-MS: 423 [M+H]+ (LC-MS 2); ESI-MS: 421 [M−H]− (LC-MS 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08975417B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-e5d944eb11b442d7aff64aff8f509d04 |
| Source note | uspto-grants-2015_03 |