huagongshe.com
HRID873979

反应详情

EQUATION

反应方程式

HRID 873979 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc(CN2C(=O)c3c(c(C)nn3-c3ccnn3C)C2c2ccc(Cl)cc2)cc1
HCID117702782

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nn(-c2ccnn2C)c2c1C(c1ccc(Cl)cc1)NC2=O
HCID117702945

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 85.6 using 4-(4-chlorophenyl)-5-(4-methoxybenzyl)-3-methyl-1-(1-methyl-1H-pyrazol-5-yl)-4,5-dihydropyrrolo-[3,4-c]pyrazol-6(1H)-one (Step 114.1). tR: 4.14 min (HPLC 1); tR: 0.92 min (LC-MS 2); ESI-MS: 328 [M+H]+ (LC-MS 2); ESI-MS: 326 [M−H]− (LC-MS 2); Rf=0.61 (EtOAc).