huagongshe.com
HRID874415

反应详情

EQUATION

反应方程式

HRID 874415 的结构方程式

REACTANTS

反应物

2
结构：C1COCCO1.Cl
HCID20443148

1,4-Dioxane hydrochloride

C4H9ClO2

结构：CC(C)(C)OC(=O)Nc1ccn2nc(Br)nc2c1
HCID67774787

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Nc1ccn2nc(Br)nc2c1
HCID117761295

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

A suspension of 4 N hydrochloric acid-1,4-dioxane (8 ml) and 1,4-dioxane (8 ml) containing the tert-butyl (2-bromo-[1,2,4]triazolo[1,5-a]pyridin-7-yl)carbamate (400 mg) obtained in (Example 3.15) <Step 4> was heated to reflux for 40 minutes.

WORKUP

后处理

  1. customobtained in (Example 3.15) <Step 4>
  2. temperaturewas heated
  3. temperatureto reflux for 40 minutes