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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 874415Generated: October 30, 2026

1,4-Dioxane hydrochloride → 1622993-13-8

https://huagongshe.com/reaction/874415

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
ReactantHCID 67774787HCID 67774787—
Solvent1,4-DioxaneHCID 31275—
Product1622993-13-8HCID 117761295—

Reaction Steps

A suspension of 4 N hydrochloric acid-1,4-dioxane (8 ml) and 1,4-dioxane (8 ml) containing the tert-butyl (2-bromo-[1,2,4]triazolo[1,5-a]pyridin-7-yl)carbamate (400 mg) obtained in (Example 3.15) <Step 4> was heated to reflux for 40 minutes.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08980889B2
Source datasetuspto-grants-2015_03
ORD IDord-c0a3b1bc301740a9a7ddbaceff9f739c
Source noteuspto-grants-2015_03