Hydrochloric Acid → HCID 90388476, compound

Participants

Reaction Steps

A mixture of Example 69b (0.25 g, 0.610 mmol) and hydrogen chloride (12.20 mL, 48.8 mmol, 4 M in dioxane) was heated at 90° C. overnight. The reaction mixture was cooled to ambient temperature, and the solvent was removed under reduced pressure to give the crude product, which was used directly for the next reaction.

Provenance & Evidence