2-Phenyl-4-carboxythiazole → HCID 46684680, compound

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Reaction Steps

This compound was synthesized from tert-butyl piperazine-1-carboxylate and 2-phenylthiazole-4-carboxylic acid as described for example 37 step 3 (500 mg, yield 90%). 1H NMR (400 MHz, DMSO-d6) δ 8.20 (s, 1H), 8.00-7.96 (m, 2H), 7.56-7.53 (m, 3H), 3.76-3.64 (m, 4H), 3.43 (m, 4H), 1.42 (s, 9H). MS (ESI) m/z: Calculated for C19H23N3O3S: 373.15. found: 374.2 (M+H)+

Provenance & Evidence