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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 875265Generated: October 30, 2026

HCID 42599313, compound → HCID 42599314, compound

https://huagongshe.com/reaction/875265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 42599313HCID 42599313—
SolventHydrochloric AcidHCID 313—
SolventEthanolHCID 702—
SolventPalladiumHCID 23938—
ProductHCID 42599314HCID 42599314—

Reaction Conditions

Temperature25 °C

Reaction Steps

Compound of example 27 (100 mg, 0.24 mmol) was dissolved in ethanol (10 mL) and to it 10% Pd/C & 10% aqueous HCl (0.1 mL) was added. The reaction mixture was stirred under hydrogen pressure for 30 hours at room temperature (25° C.). The reaction mixture was filtered over celite and concentrated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08981131B2
Source datasetuspto-grants-2015_03
ORD IDord-ee3e0b883b464427bce7198a86453008
Source noteuspto-grants-2015_03