HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 53261255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 63587641 | HCID 63587641 | — |
| Product | HCID 53261255 | HCID 53261255 | 73% |
Reaction Steps
A mixture of 130 mg of 6-chloro-N-(4-phenoxyphenyl)pyridin-2-amine in 214 mg of ethanolamine was filled in a screw cap vial and was treated analogously to the method as set out in Example 16b, but using for flash column chromatography a solvent mixture of EtOAc:PE=1:1 instead of EtOAc:PE=3:1). 2-(6-(4-Phenoxyphenylamino)pyridin-2-ylamino)ethan-1-ol was obtained in the form of a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08986994B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-87d6a40ea22d4dc1b1b52bfae72ed37c |
| Source note | uspto-grants-2015_03 |