HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66701425, compound → HCID 66701320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66701425 | HCID 66701425 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 66701320 | HCID 66701320 | — |
Reaction Steps
A solution of 1.0 g (4.7 mmol) of 3-(4-ethylphenyl)-5-methoxypyridine in 120 ml of acetic acid was reacted according to General Method 5A. The solution was concentrated under reduced pressure. The crude product was purified by flash chromatography (silica gel, dichloromethane/methanol gradient). Yield: 880 mg (86% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987248B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-64950271b4e84d9f99ebabaea811eaa9 |
| Source note | uspto-grants-2015_03 |