反应详情

A solution of 550 mg (1.82 mmol) of N-[5-(2,3-dimethylphenyl)pyridin-3-yl]benzamide in 150 ml of ethanol was reacted according to General Method 5A. The solution was concentrated under reduced pressure. The product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient). Yield: 760 mg (77% of theory, purity 57%)

1. concentrationThe solution was concentrated under reduced pressure
2. customThe product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient)