反应详情

A solution of 840 mg (1.82 mmol) of N-{5-[3-(trifluoromethyl)phenyl]pyridin-3-yl]benzamide in 100 ml of glacial acetic acid was reacted according to General Method 6A. The solution was concentrated under reduced pressure. The product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient). Yield: 700 mg

1. concentrationThe solution was concentrated under reduced pressure
2. customThe product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient)