反应详情

A solution of 1.0 g (2.9 mmol) of N-{5-[4-(trifluoromethyl)phenyl]pyridin-3-yl]benzamide in 120 ml of glacial acetic acid was reacted according to General Method 6A. The solution was concentrated under reduced pressure. The product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient). Yield: 657 mg (50% pure).

1. concentrationThe solution was concentrated under reduced pressure
2. customThe product was purified by preparative HPLC (Reprosil C18, water/acetonitrile gradient)