Hydrochloric Acid → HCID 67222333, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of compound 18-2 (0.34 g) in MeOH (10.2 mL), was added K2CO3 (272 mg) at 0° C. The reaction mixture was stirred at 0° C. overnight. Then 1N HCl (2 mL), H2O (5 mL) and Et2O (15 mL) were added into the reaction mixture. The precipitate was collected by filtration and was rinsed with H2O and Et2O to obtain compound 18-3 (40 mg) as a colorless amorphous solid.

Provenance & Evidence