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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 876577Generated: November 1, 2026

HCID 67222305, compound → HCID 58181897, compound

https://huagongshe.com/reaction/876577

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67222305HCID 67222305—
CatalystPalladiumHCID 23938—
SolventMeOH tetrahydrofuranHCID 21899815—
ProductHCID 58181897HCID 5818189797.8%

Reaction Steps

To a solution of compound 39-1 (0.3 g) in MeOH-THF (3 mL-3 mL), was added 10% Pd/C (30 mg). The reaction mixture was stirred under hydrogen atmosphere for 3 hours at room temperature. Then the reaction mixture was filtered with Celite® pad to remove catalyst. The filtrate was concentrated in vacuo to obtain compound 39-2 (0.27 g) as pale brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08987242B2
Source datasetuspto-grants-2015_03
ORD IDord-1abb17ad1e6b47ab9540db3775b419d7
Source noteuspto-grants-2015_03