HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 86653953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 67223362 | HCID 67223362 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86653953 | HCID 86653953 | — |
Reaction Steps
To a suspension of compound 66-1 (60 mg) in EtOH (2 mL), was added 50% NH2OH aq. (22.4 microL). The reaction mixture was stirred at room temperature overnight. Then the mixture was concentrated in vacuo to obtain compound 66-2 (67 mg) as a colorless amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987242B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-35852d5b1e154766af4620bc6069db2b |
| Source note | uspto-grants-2015_03 |