HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-2-N-Boc-1,2,3,4-tetrahydro-isoquinoline → HCID 67222175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-2-N-Boc-1,2,3,4-tetrahydro-isoquinoline | HCID 2756371 | — |
| Reactant | HCID 58181678 | HCID 58181678 | — |
| Product | HCID 67222175 | HCID 67222175 | 72.6% |
Reaction Steps
According to the Step 70-5 in the synthetic method for EXAMPLE 70, compound 70-4 (50 mg) was treated with tert-butyl 6-amino-3,4-dihydroisoquinoline-2(1H)-carboxylate (30 mg) to afford compound 72-1 (52 mg) as a light yellow solid after preparative LC purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987242B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-fea3549c8c06443da1351811b3d7576f |
| Source note | uspto-grants-2015_03 |