HRID876609

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2733960

Thiophene-2-boronic acid

C4H5BO2S

HCID2773539

2-(Methylsulfonyl)phenylboronic acid

C7H9BO4S

结构：CC(C)(C)OC(=O)[C@H](O)[C@H]1OCCN(c2ccc(I)cc2)C1=O

HCID67223457

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)[C@H](O)[C@H]1OCCN(c2ccc(-c3ccccc3S(C)(=O)=O)cc2)C1=O

HCID67223107

未命名化合物

收率 79.8%

PROCEDURE

实验过程

According to the Step 22-1 in synthetic method for EXAMPLE 22, compound 105-1 (0.12 g) and 2-methylsulfonylphenylboronic acid (0.11 g) were used instead of 14-4 and 2-thiopheneboronic acid to obtain compound 105-2 (102 mg) as yellow oil.