HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 876635Generated: October 30, 2026
N-bromobutanimide → HCID 58290597, compound
https://huagongshe.com/reaction/876635
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 3-Amino-5-methylbenzotrifluoride | HCID 2737713 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58290597 | HCID 58290597 | — |
Reaction Steps
3-methyl-5-(trifluoromethyl)aniline (4.84 g, 0.011 mol) was dissolved in CH2Cl2 and cooled to 0° C. NBS (4.92 g, 1 eq) was added and the mixture stirred overnight. The reaction mixture was loaded onto silica gel and eluted with 0-20% EtOAc in hexane to give 2.3 g of M21-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08987242B2 |
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| Source dataset | uspto-grants-2015_03 |
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| ORD ID | ord-7f2428c7e38144a08fcf485fcc641492 |
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| Source note | uspto-grants-2015_03 |
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