HRID877180

反应详情

EQUATION

反应方程式

HRID 877180 的结构方程式

PROCEDURE

实验过程

246 mg (0.766 mmol) of [4-(bromomethyl)phenyl](cyclopentyl)acetic acid were dissolved in 5 ml of thionyl chloride, and the mixture was stirred at room temperature for 1 h and then at 50° C. for 1 h. The mixture was then concentrated under reduced pressure. This gave 253 mg of the title compound, which was reacted without further purification in the next step.

WORKUP

后处理

  1. waitat 50° C. for 1 h
  2. concentrationThe mixture was then concentrated under reduced pressure
  3. customThis gave 253 mg of the title compound, which was reacted without further purification in the next step