HRID877180
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
246 mg (0.766 mmol) of [4-(bromomethyl)phenyl](cyclopentyl)acetic acid were dissolved in 5 ml of thionyl chloride, and the mixture was stirred at room temperature for 1 h and then at 50° C. for 1 h. The mixture was then concentrated under reduced pressure. This gave 253 mg of the title compound, which was reacted without further purification in the next step.
WORKUP
后处理
- waitat 50° C. for 1 h
- concentrationThe mixture was then concentrated under reduced pressure
- customThis gave 253 mg of the title compound, which was reacted without further purification in the next step