HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 7-Bromo-4-phenylbenz[a]anthracene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 4-Phenylbenz[a]anthracene | HCID 59412490 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 7-Bromo-4-phenylbenz[a]anthracene | HCID 59412769 | — |
Reaction Steps
16.9 g (95 mmol) of N-bromosuccinimide are added at 100° C. to a suspension of 18.2 g (45 mmol) of 4-phenylbenz[a]anthracene in 500 ml of DMF. After 3 h, 500 ml of ethanol are added at room temperature, and the solid is filtered off with suction, washed with ethanol and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08986852B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-6ff75dd2df164416935a2a436a299fe0 |
| Source note | uspto-grants-2015_03 |