反应详情

16.9 g (95 mmol) of N-bromosuccinimide are added at 100° C. to a suspension of 18.2 g (45 mmol) of 4-phenylbenz[a]anthracene in 500 ml of DMF. After 3 h, 500 ml of ethanol are added at room temperature, and the solid is filtered off with suction, washed with ethanol and dried.

1. filtrationthe solid is filtered off with suction
2. washwashed with ethanol
3. customdried