HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 59412614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 59412708 | HCID 59412708 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59412614 | HCID 59412614 | — |
Reaction Steps
20 g (116 mmol) of N-bromosuccinimide are added at 100° C. to a suspension of 55 g (116 mmol) of 4-(9-phenylanthracen-10-yl)benz[a]anthracene in 500 ml of DMF. After 3 h, 500 ml of ethanol are added at room temperature, and the solid is filtered off with suction, washed with ethanol and dried. Yield: 63 g (113 mmol), 65%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08986852B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-b0540b763a384e68866a90a40eecf424 |
| Source note | uspto-grants-2015_03 |