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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 877301Generated: October 29, 2026

Ethanol → HCID 59412614, compound

https://huagongshe.com/reaction/877301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 59412708HCID 59412708—
SolventDimethylformamideHCID 6228—
ProductHCID 59412614HCID 59412614—

Reaction Steps

20 g (116 mmol) of N-bromosuccinimide are added at 100° C. to a suspension of 55 g (116 mmol) of 4-(9-phenylanthracen-10-yl)benz[a]anthracene in 500 ml of DMF. After 3 h, 500 ml of ethanol are added at room temperature, and the solid is filtered off with suction, washed with ethanol and dried. Yield: 63 g (113 mmol), 65%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08986852B2
Source datasetuspto-grants-2015_03
ORD IDord-b0540b763a384e68866a90a40eecf424
Source noteuspto-grants-2015_03