HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86668958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67170071 | HCID 67170071 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86668958 | HCID 86668958 | — |
Reaction Steps
To a solution of 0.71 g (1.9 mmol) N-[(S)-(4-bromophenyl)(1-methyl-1H-1,2,3-triazol-4-yl)methyl]-2-methylpropane-2-sulfinamide in 5.0 ml MeOH was added 1.4 mL (2.8 mmol) 2.0M HCl in diethyl ether. After 30 min at room temperature, the reaction mixture was concentrated in vacuo to afford (S)-(4-bromophenyl)(1-methyl-1H-1,2,3-triazol-4-yl)methanaminium chloride. ES-MS [M+1]+=269.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08987310B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-af5a2c5950724e5db7ad3e247fd442c0 |
| Source note | uspto-grants-2015_03 |