Hydrochloric Acid → HCID 178491234, compound

Participants

Reaction Steps

To a solution of N-[(4-methoxyphenyl)(2-methyl-1H-imidazol-4-yl)methyl]-2-methylpropane-2-sulfinamide (0.735 mg, 2.287 mmol) in 10.0 ml of MeOH was added 2.0N HCl in Et2O (11.43 ml, 22.87 mmol), and the mixture was stirred at RT for 30 min. Solvent removed and the residue was dried under vacuum to give the crude title compound (0.568 g, 98%). ES-MS [M+1]+: m/z 218.1. This intermediate was carried over to the next step without further purification and characterization.

Provenance & Evidence