反应详情

温度

60 °C

After 21.2 g (0.20 mol) of sodium carbonate and 20.0 g (0.10 mol) of cyanuric chloride were added and dissolved into 140 g of 1,4-dioxane, 19.8 g (0.20 mol) of diallylamine was gradually added thereinto and further, 8.4 g (0.20 mol) of caustic soda was added thereinto. By generating the heat of reaction, the temperature of reaction solution was raised to about 60° C. and the reaction was continued at the temperature for 2 hours. Thereafter, the reaction mixture was cooled and filtered to remove the sodium chloride generated as the byproduct. The obtained filtrate was distilled under reduced pressure to recover the solvent. Therefore, 34 g (0.09 mol) of 4,6-bis(diallylamino)-2-chloro-1,3,5-triazine was obtained.

1. additionwas gradually added
2. temperatureheat of reaction
3. customthe temperature of reaction solution
4. temperatureThereafter, the reaction mixture was cooled
5. filtrationfiltered
6. customto remove the sodium chloride
7. distillationThe obtained filtrate was distilled under reduced pressure
8. customto recover the solvent