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HRID878034

反应详情

EQUATION

反应方程式

HRID 878034 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1cc(C(F)(F)F)cc(C(F)(F)F)c1
HCID101856

3,5-Bis(trifluoromethyl)benzoyl chloride

C9H3ClF6O

结构：CNc1cnccc1-c1ccnc(Cl)c1F
HCID86670705

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)c1cc(C(F)(F)F)cc(C(F)(F)F)c1)c1cnccc1-c1ccnc(Cl)c1F
HCID60197498

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to example 55, from (2′-chloro-3′-fluoro-[4,4]bipyridinyl-3-yl)-methyl-amine and 3,5-bis(trifluoromethyl)benzoyl chloride (CAS RN 1271-19-8) and using preparative HPLC for the chromatographic purification. Off-white solid (12%). MS (ESI): m/z=478.0 [M+H]+.

WORKUP

后处理

  1. customfor the chromatographic purification