HRID878040

反应详情

EQUATION

反应方程式

HRID 878040 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in analogy to example 58, from N-(4-bromo-pyridin-3-yl)-N-methyl-3,5-bis-trifluoromethyl-benzamide (example 25, intermediate a) and 2-methoxy-3,4-difluorophenylboronic acid (CAS RN 905583-06-4) and using preparative HPLC for the chromatographic purification. Off-white solid (49%). MS (ESI): m/z=491.1 [M+H]+.

WORKUP

后处理

  1. customfor the chromatographic purification